An Introductory Course of Quantitative Chemical Analysis With Explanatory Notes
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AN INTRODUCTORY COURSE
BY
PREFACE
CONTENTS
PART I. INTRODUCTION
PART II. VOLUMETRIC ANALYSIS
PART III. GRAVIMETRIC ANALYSIS
PART II. VOLUMETRIC ANALYSIS
PART III. GRAVIMETRIC ANALYSIS
QUANTITATIVE CHEMICAL ANALYSIS
PART I
GENERAL DIRECTIONS
ACCURACY AND ECONOMY OF TIME
NOTEBOOKS
REAGENTS
WASH-BOTTLES
TRANSFER OF LIQUIDS
EVAPORATION OF LIQUIDS
NOTEBOOKS
REAGENTS
WASH-BOTTLES
TRANSFER OF LIQUIDS
EVAPORATION OF LIQUIDS
PART II
MEASURING INSTRUMENTS
THE ANALYTICAL BALANCE
WEIGHTS
BURETTES
PREPARATION OF A BURETTE FOR USE
READING OF A BURETTE
CALIBRATION OF GLASS MEASURING DEVICES
CALIBRATION OF THE BURETTES
PIPETTES
CALIBRATION OF PIPETTES
FLASKS
GRADUATION OF FLASKS
THE ANALYTICAL BALANCE
WEIGHTS
BURETTES
PREPARATION OF A BURETTE FOR USE
READING OF A BURETTE
CALIBRATION OF GLASS MEASURING DEVICES
CALIBRATION OF THE BURETTES
PIPETTES
CALIBRATION OF PIPETTES
FLASKS
GRADUATION OF FLASKS
GENERAL DIRECTIONS FOR VOLUMETRIC ANALYSES
STANDARD SOLUTIONS
NORMAL SOLUTIONS
NORMAL SOLUTIONS
I. NEUTRALIZATION METHODS
GENERAL DISCUSSION
INDICATORS
BEHAVIOR OF ORGANIC INDICATORS
PREPARATION OF INDICATOR SOLUTIONS
PREPARATION OF STANDARD SOLUTIONS
COMPARISON OF ACID AND ALKALI SOLUTIONS
BEHAVIOR OF ORGANIC INDICATORS
PREPARATION OF INDICATOR SOLUTIONS
PREPARATION OF STANDARD SOLUTIONS
COMPARISON OF ACID AND ALKALI SOLUTIONS
STANDARDIZATION OF HYDROCHLORIC ACID
STANDARDIZATION
DETERMINATION OF THE TOTAL ALKALINE STRENGTH OF SODA ASH
DETERMINATION OF THE ACID STRENGTH OF OXALIC ACID
II. OXIDATION PROCESSES
BICHROMATE PROCESS FOR THE DETERMINATION OF IRON
NORMAL SOLUTIONS OF OXIDIZING OR REDUCING AGENTS
PREPARATION OF SOLUTIONS
INDICATOR SOLUTION
COMPARISON OF OXIDIZING AND REDUCING SOLUTIONS
STANDARDIZATION OF POTASSIUM BICHROMATE SOLUTIONS
STANDARDIZATION
PREPARATION OF SOLUTIONS
INDICATOR SOLUTION
COMPARISON OF OXIDIZING AND REDUCING SOLUTIONS
STANDARDIZATION OF POTASSIUM BICHROMATE SOLUTIONS
STANDARDIZATION
DETERMINATION OF IRON IN LIMONITE
DETERMINATION OF CHROMIUM IN CHROME IRON ORE
PERMANGANATE PROCESS FOR THE DETERMINATION OF IRON
PREPARATION OF A STANDARD SOLUTION
COMPARISON OF PERMANGANATE AND FERROUS SOLUTIONS
STANDARDIZATION OF A POTASSIUM PERMANGANATE SOLUTION
STANDARDIZATION
COMPARISON OF PERMANGANATE AND FERROUS SOLUTIONS
STANDARDIZATION OF A POTASSIUM PERMANGANATE SOLUTION
STANDARDIZATION
DETERMINATION OF IRON IN LIMONITE
DETERMINATION OF THE OXIDIZING POWER OF PYROLUSITE
IODIMETRY
PREPARATION OF STANDARD SOLUTIONS
INDICATOR SOLUTION
COMPARISON OF IODINE AND THIOSULPHATE SOLUTIONS
STANDARDIZATION OF SOLUTIONS
INDICATOR SOLUTION
COMPARISON OF IODINE AND THIOSULPHATE SOLUTIONS
STANDARDIZATION OF SOLUTIONS
DETERMINATION OF COPPER IN ORES
DETERMINATION OF ANTIMONY IN STIBNITE
CHLORIMETRY
DETERMINATION OF THE AVAILABLE CHLORINE IN BLEACHING POWDER
III. PRECIPITATION METHODS
DETERMINATION OF SILVER BY THE THIOCYANATE PROCESS
STANDARDIZATION
DETERMINATION OF SILVER IN COIN
DETERMINATION OF SILVER IN COIN
PART III
GENERAL DIRECTIONS
PRECIPITATION
FUNNELS AND FILTERS
FILTRATION AND WASHING OF PRECIPITATES
DESICCATORS
CRUCIBLES
PREPARATION OF CRUCIBLES FOR USE
IGNITION OF PRECIPITATES
FUNNELS AND FILTERS
FILTRATION AND WASHING OF PRECIPITATES
DESICCATORS
CRUCIBLES
PREPARATION OF CRUCIBLES FOR USE
IGNITION OF PRECIPITATES
DETERMINATION OF CHLORINE IN SODIUM CHLORIDE
DETERMINATION OF IRON AND OF SULPHUR IN FERROUS AMMONIUM SULPHATE,
DETERMINATION OF IRON
DETERMINATION OF SULPHUR
DETERMINATION OF SULPHUR IN BARIUM SULPHATE
DETERMINATION OF PHOSPHORIC ANHYDRIDE IN APATITE
PRECIPITATION OF AMMONIUM PHOSPHOMOLYBDATE
PRECIPITATION OF MAGNESIUM AMMONIUM PHOSPHATE
REPRECIPITATION AND IGNITION OF MAGNESIUM AMMONIUM PHOSPHATE
PRECIPITATION OF MAGNESIUM AMMONIUM PHOSPHATE
REPRECIPITATION AND IGNITION OF MAGNESIUM AMMONIUM PHOSPHATE
ANALYSIS OF LIMESTONE
DETERMINATION OF MOISTURE
DETERMINATION OF FERRIC OXIDE AND ALUMINIUM OXIDE (WITH MANGANESE)
DETERMINATION OF CALCIUM
DETERMINATION OF MAGNESIUM
DETERMINATION OF CARBON DIOXIDE
DETERMINATION OF LEAD, COPPER, IRON, AND ZINC IN BRASS
DETERMINATION OF COPPER AND LEAD
DETERMINATION OF IRON
DETERMINATION OF ZINC
DETERMINATION OF SILICA IN SILICATES
PREPARATION OF THE SAMPLE
FUSION AND SOLUTION
DEHYDRATION AND FILTRATION
IGNITION AND TESTING OF SILICA
FUSION AND SOLUTION
DEHYDRATION AND FILTRATION
IGNITION AND TESTING OF SILICA
PART IV
PROBLEMS
VOLUMETRIC ANALYSIS
GRAVIMETRIC ANALYSIS
GRAVIMETRIC ANALYSIS
APPENDIX
ELECTROLYTIC DISSOCIATION THEORY
THE FOLDING OF A FILTER PAPER
!SAMPLE PAGES FOR LABORATORY RECORDS!
STRENGTH OF REAGENTS
CORRECTIONS FOR CHANGE OF TEMPERATURE OF STANDARD SOLUTIONS
!SAMPLE PAGES FOR LABORATORY RECORDS!
STRENGTH OF REAGENTS
CORRECTIONS FOR CHANGE OF TEMPERATURE OF STANDARD SOLUTIONS
INTERNATIONAL ATOMIC WEIGHTS
INDEX
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