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An Introductory Course of Quantitative Chemical Analysis With Explanatory Notes

By Henry Paul Talbot

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Table of Contents

AN INTRODUCTORY COURSE
BY
PREFACE
CONTENTS
- PART I. INTRODUCTION
  - PART II. VOLUMETRIC ANALYSIS
  - PART III. GRAVIMETRIC ANALYSIS
- PART II. VOLUMETRIC ANALYSIS
- PART III. GRAVIMETRIC ANALYSIS
QUANTITATIVE CHEMICAL ANALYSIS
PART I
GENERAL DIRECTIONS
- ACCURACY AND ECONOMY OF TIME
  - NOTEBOOKS
  - REAGENTS
  - WASH-BOTTLES
  - TRANSFER OF LIQUIDS
  - EVAPORATION OF LIQUIDS
- NOTEBOOKS
- REAGENTS
- WASH-BOTTLES
- TRANSFER OF LIQUIDS
- EVAPORATION OF LIQUIDS
PART II
- MEASURING INSTRUMENTS
  - THE ANALYTICAL BALANCE
  - WEIGHTS
  - BURETTES
  - PREPARATION OF A BURETTE FOR USE
  - READING OF A BURETTE
  - CALIBRATION OF GLASS MEASURING DEVICES
  - CALIBRATION OF THE BURETTES
  - PIPETTES
  - CALIBRATION OF PIPETTES
  - FLASKS
  - GRADUATION OF FLASKS
- THE ANALYTICAL BALANCE
- WEIGHTS
- BURETTES
- PREPARATION OF A BURETTE FOR USE
- READING OF A BURETTE
- CALIBRATION OF GLASS MEASURING DEVICES
- CALIBRATION OF THE BURETTES
- PIPETTES
- CALIBRATION OF PIPETTES
- FLASKS
- GRADUATION OF FLASKS
GENERAL DIRECTIONS FOR VOLUMETRIC ANALYSES
- STANDARD SOLUTIONS
  - NORMAL SOLUTIONS
- NORMAL SOLUTIONS
I. NEUTRALIZATION METHODS
GENERAL DISCUSSION
- INDICATORS
  - BEHAVIOR OF ORGANIC INDICATORS
  - PREPARATION OF INDICATOR SOLUTIONS
  - PREPARATION OF STANDARD SOLUTIONS
  - COMPARISON OF ACID AND ALKALI SOLUTIONS
- BEHAVIOR OF ORGANIC INDICATORS
- PREPARATION OF INDICATOR SOLUTIONS
- PREPARATION OF STANDARD SOLUTIONS
- COMPARISON OF ACID AND ALKALI SOLUTIONS
STANDARDIZATION OF HYDROCHLORIC ACID
- STANDARDIZATION
DETERMINATION OF THE TOTAL ALKALINE STRENGTH OF SODA ASH
DETERMINATION OF THE ACID STRENGTH OF OXALIC ACID
II. OXIDATION PROCESSES
BICHROMATE PROCESS FOR THE DETERMINATION OF IRON
- NORMAL SOLUTIONS OF OXIDIZING OR REDUCING AGENTS
  - PREPARATION OF SOLUTIONS
  - INDICATOR SOLUTION
  - COMPARISON OF OXIDIZING AND REDUCING SOLUTIONS
  - STANDARDIZATION OF POTASSIUM BICHROMATE SOLUTIONS
  - STANDARDIZATION
- PREPARATION OF SOLUTIONS
- INDICATOR SOLUTION
- COMPARISON OF OXIDIZING AND REDUCING SOLUTIONS
- STANDARDIZATION OF POTASSIUM BICHROMATE SOLUTIONS
- STANDARDIZATION
DETERMINATION OF IRON IN LIMONITE
DETERMINATION OF CHROMIUM IN CHROME IRON ORE
PERMANGANATE PROCESS FOR THE DETERMINATION OF IRON
- PREPARATION OF A STANDARD SOLUTION
  - COMPARISON OF PERMANGANATE AND FERROUS SOLUTIONS
  - STANDARDIZATION OF A POTASSIUM PERMANGANATE SOLUTION
  - STANDARDIZATION
- COMPARISON OF PERMANGANATE AND FERROUS SOLUTIONS
- STANDARDIZATION OF A POTASSIUM PERMANGANATE SOLUTION
- STANDARDIZATION
DETERMINATION OF IRON IN LIMONITE
DETERMINATION OF THE OXIDIZING POWER OF PYROLUSITE
IODIMETRY
- PREPARATION OF STANDARD SOLUTIONS
  - INDICATOR SOLUTION
  - COMPARISON OF IODINE AND THIOSULPHATE SOLUTIONS
  - STANDARDIZATION OF SOLUTIONS
- INDICATOR SOLUTION
- COMPARISON OF IODINE AND THIOSULPHATE SOLUTIONS
- STANDARDIZATION OF SOLUTIONS
DETERMINATION OF COPPER IN ORES
DETERMINATION OF ANTIMONY IN STIBNITE
CHLORIMETRY
DETERMINATION OF THE AVAILABLE CHLORINE IN BLEACHING POWDER
III. PRECIPITATION METHODS
DETERMINATION OF SILVER BY THE THIOCYANATE PROCESS
- STANDARDIZATION
  - DETERMINATION OF SILVER IN COIN
- DETERMINATION OF SILVER IN COIN
PART III
GENERAL DIRECTIONS
- PRECIPITATION
  - FUNNELS AND FILTERS
  - FILTRATION AND WASHING OF PRECIPITATES
  - DESICCATORS
  - CRUCIBLES
  - PREPARATION OF CRUCIBLES FOR USE
  - IGNITION OF PRECIPITATES
- FUNNELS AND FILTERS
- FILTRATION AND WASHING OF PRECIPITATES
- DESICCATORS
- CRUCIBLES
- PREPARATION OF CRUCIBLES FOR USE
- IGNITION OF PRECIPITATES
DETERMINATION OF CHLORINE IN SODIUM CHLORIDE
DETERMINATION OF IRON AND OF SULPHUR IN FERROUS AMMONIUM SULPHATE,
- DETERMINATION OF IRON
DETERMINATION OF SULPHUR
DETERMINATION OF SULPHUR IN BARIUM SULPHATE
DETERMINATION OF PHOSPHORIC ANHYDRIDE IN APATITE
- PRECIPITATION OF AMMONIUM PHOSPHOMOLYBDATE
  - PRECIPITATION OF MAGNESIUM AMMONIUM PHOSPHATE
  - REPRECIPITATION AND IGNITION OF MAGNESIUM AMMONIUM PHOSPHATE
- PRECIPITATION OF MAGNESIUM AMMONIUM PHOSPHATE
- REPRECIPITATION AND IGNITION OF MAGNESIUM AMMONIUM PHOSPHATE
ANALYSIS OF LIMESTONE
- DETERMINATION OF MOISTURE
DETERMINATION OF FERRIC OXIDE AND ALUMINIUM OXIDE (WITH MANGANESE)
DETERMINATION OF CALCIUM
DETERMINATION OF MAGNESIUM
DETERMINATION OF CARBON DIOXIDE
DETERMINATION OF LEAD, COPPER, IRON, AND ZINC IN BRASS
DETERMINATION OF COPPER AND LEAD
DETERMINATION OF IRON
DETERMINATION OF ZINC
DETERMINATION OF SILICA IN SILICATES
- PREPARATION OF THE SAMPLE
  - FUSION AND SOLUTION
  - DEHYDRATION AND FILTRATION
  - IGNITION AND TESTING OF SILICA
- FUSION AND SOLUTION
- DEHYDRATION AND FILTRATION
- IGNITION AND TESTING OF SILICA
PART IV
PROBLEMS
- VOLUMETRIC ANALYSIS
  - GRAVIMETRIC ANALYSIS
- GRAVIMETRIC ANALYSIS
APPENDIX
- ELECTROLYTIC DISSOCIATION THEORY
- THE FOLDING OF A FILTER PAPER
  - !SAMPLE PAGES FOR LABORATORY RECORDS!
  - STRENGTH OF REAGENTS
  - CORRECTIONS FOR CHANGE OF TEMPERATURE OF STANDARD SOLUTIONS
- !SAMPLE PAGES FOR LABORATORY RECORDS!
- STRENGTH OF REAGENTS
- CORRECTIONS FOR CHANGE OF TEMPERATURE OF STANDARD SOLUTIONS
- INTERNATIONAL ATOMIC WEIGHTS
INDEX
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